in-situ Atomic-Force-Microscopy
in Transmission-Electron-Microscopy

Summary:
When the lateral displacement of the tip (see Fig.1) is comparable or larger than the scan area size, for example at atomic-scale friction, the interpretation of friction image is changed from the case that the scan size is much larger than the lateral displacement of the tip. The same situation occurs in contact mode surface corrugation measurement. This is because, by the lateral displacement of the tip, the tip is not at the position where the raster scan points, which is clearly observed by an in-situ TEM/AFM combined microscopy and atomic-scale friction analysis by two-dimensional stick-slip model. Moreover, the lateral displacement of the tip, i.e. friction at the order of nm scale creates the hysteresis in the force-distance relation curve behavior, as shown in Fig.2.

Fig.1: Lateral displacement along Y direction is generated by the Z direction force. This means that the AFM tip slides along surface during force-distance curve!

Fig.2: A typical force-distance relation curve of AFM shows the hysteresis, which is caused by the lateral displacement of the tip.

---> Application of TEM/AFM/STM (1) - Data Movie with Atomic Resolution

Simultaneous Observation of Millisecond Dynamics in Atomistic Structure, Stress-Strain Curve , Conductance, and Force of Au Nanowire under Tensile Strength Test

---> Award (in Japan)

---> Publication

---> Application of TEM/AFM/STM (2) - Data Movie with Atomic Resolution

Sigle Atom Wire of Au

---> Publication

---> Application of TEM/AFM/ (3) - Force Curve Movie with Atomic Resolution

Force Curve of SiO tip on SiO surface

Publications:

1

"Effect of Lateral Displacement of Atomic Force Microscope Tip Caused by Contact Scanning Studied with In-Situ Transmission Electron Microscopy"S. Fujisawa and T. Kizuka, Japanese Journal of Applied Physics, vol.42, pp.L1182-L1184 (2003).

2

"Lateral Displacement of an AFM Tip Observed by In-Situ TEM/AFM Combined Microscopy: The Effect of the Friction in AFM" S. Fujisawa and T. Kizuka, Tribology Letters, vol.15, pp.163-168 (2003).

3

"Simultaneous observation of millisecond dynamics in atomistic structure, force and conductance on the basis of transmission electron microscope" T.Kizuka, H.Ohmi, T.Sumi, K.Kumazawa, S.Deguchi, M.Naruse, S.Fujisawa, S.Sasaki, A.Yabe and Y.Enomoto, Japanese Journal of Applied Physics, vol.40, pp.L170-L173 (2001).

Back to Research by Satoru FUJISAWA